MARUM
-
Sediment Geochemistry
-
Leobener Str
-
D-28359 Bremen
- Germany
Marine Geochemistry - Laboratory Methods
Pb - Lead
sample ty
pe
marine porewater
digested sediment 1g/L
groundwater
typical concentration
0.5 µmol/L
100 ppb
500 µmol/L
100 ppm
0.02 µmol/L
5 ppb
Method1
ICP-OES
wavelength
220.353 nm ->
wavelength table
method used
no
yes
no
dilution
no
sample size
> 2 mL
detction limit
100 ppb
standard solutions
Single element standard in nitric acid 1%
Method 2
GF-AAS
wavelength
217.0 nm
method used
no
yes
yes
dilution
1:1000
1:10
sample size
500 µL
500 µL
detction limit
1 ppb
1 ppb
standard solutions
Single element standard in nitric acid 1%
Single element standard in nitric acid 1%
Method 3
ICP-MS
Mass
208 ->
Mass Table
method used
yes
yes
yes
dilution
1:100
1:100
1:10
sample size
> 1 mL
> 1 mL
> 1mL
detction limit
100 ppb
100 ppb
1 ppb
standard solutions
Multielement standard in nitric acid 1%
M4
,
M6
,
Kraft ME
Multielement standard in nitric acid 1%
M4
,
M6
,
Kraft ME
Multielement standard in nitric acid 1%
M4
,
M6
,
Kraft ME
tips + tricks
page created by
M.Kölling
& T.Feseker