core
segments are stored at 4°C until sampling |
|
labeled core liner is cut in cool lab using an oscillating saw |
|
the cut core
segment is transferred into the argon- flooded glovebox through
the shutter. the two halves are separated inside the box using a
string and the archive half is taken out again for further documentation
(photographs, color scanning) and conductivity measurements
|
|
work half of
the core segment inside the glove box.
Eh and pH measurement
are performed using punch-in electrodes. Sediment samples are taken
at defined depths and transferred into PTFE pressure filtration
device.
|
|
small
version of the pressure filtration device. The lowermost chamber is
filled with sediment |
|
all six chambers
of one pressure filtration device are filled and attached to argon
distributor valves. The drain tubes are connected to 20 ml PE scintillation
vials. Instruments for Eh and pH measurement are situated on top
of the glovebox while electrodes remain inside. Usually two scientists
work in the cool lab
|
|
|
Samples
for dissolved iron analysis are pipetted
into 2ml Eppendorf cups prepared with color reagent (or directly into
sealable cuvettes) within the glovebox. We use 0,2 µm Filter
(i.e.Sartorius
# 11107-142) for pressure filtration. |